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Beilstein J. Org. Chem. 2024, 20, 823–829, doi:10.3762/bjoc.20.74
Graphical Abstract
Figure 1: Previous work on migration reactions in 6,8-dioxabicyclooctan-4-ols [18].
Scheme 1: Structures for 10a–c, preparation of 10d–f, and X-ray structure of 10e.
Scheme 2: Rearrangement reactions for 10a–f promoted by SOCl2.
Scheme 3: Reactions of allylic alcohols 15 and 18 with SOCl2.
Scheme 4: Appel reactions of dioxabicyclo[3.2.1]octan-4-ols 10a,e,f and 15.
Scheme 5: Some transformations for the skeletal rearrangement products 11a and 12a and X-ray structure for 24....
Figure 2: Mechanism for the rearrangement of 10, and Newman projection and the X-ray structure of 10d project...
Beilstein J. Org. Chem. 2012, 8, 71–80, doi:10.3762/bjoc.8.7
Figure 1: The structures of a) the parent [3]-, [4]-, [5]-, and [6]dendralenes and b) the corresponding radia...
Scheme 1: Synthesis of (a) hexakis(3-cyanophenyl)[3]radialene (2) and (b) hexakis(3,4-dicyanophenyl)[3]radial...
Figure 2: A perspective view of the asymmetric unit of 3.
Figure 3: (a) UV–visible (bold line) and fluorescence (dashed line) spectra of 1, 2, hexa(2-pyridyl)[3]radial...